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1 article(s) from Ahrens, Mike

Activation of pentafluoropropane isomers at a nanoscopic aluminum chlorofluoride: hydrodefluorination versus dehydrofluorination

Maëva-Charlotte Kervarec,
Thomas Braun,
Mike Ahrens and
Erhard Kemnitz

Beilstein J. Org. Chem. 2020, 16, 2623–2635, doi:10.3762/bjoc.16.213

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Scheme 1: Reactivity of tetrafluoropropanes HFO-1234yf (1) (top) and HFO-1234ze (4a) (bottom) in the presence...

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Scheme 2: Reactivity of 10a in the presence of ACF as the catalyst in C₆D₁₂ (top) or C₆D₆ (bottom) as solvent...

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Scheme 3: Proposed catalytic cycle of the transformation of 10a in C₆D₁₂ and C₆D₆ in the presence of ACF as t...

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Scheme 4: Reactivity of 10a in the presence of ACF as the catalyst and HSiEt₃ as a hydrogen source in C₆D₁₂ (...

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Scheme 5: Proposed catalytic cycle for sylilium-mediated hydrodefluorinations and dehydrofluorinations from 1...

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Scheme 6: Reactivity of 13 in the presence of ACF as the catalyst, with (top) or without (bottom) HSiEt₃ as a...

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Scheme 7: Independent reactions starting from 5, 6, or 14 in the presence of ACF as the catalyst.

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Scheme 8: Proposed reaction pathways starting from 10a in the presence of ACF and silane.

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Scheme 9: Reactivity of 10c in the presence of ACF as the catalyst and 0.5 equivalents of HSiEt₃ as a hydroge...

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Scheme 10: Proposed catalytic cycles for the transformation of 10c in C₆D₁₂ and in the presence of 0.5 equival...

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Scheme 11: Reactivity of 10c in the presence of ACF as the catalyst and HSiEt₃ as a hydrogen source in C₆D₁₂ (...

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Scheme 12: Proposed reaction pathways starting from 10c in the presence of ACF and silane.

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Scheme 13: Reactivity of 10b in the presence of ACF as the catalyst and HSiEt₃ as a hydrogen source in C₆D₁₂ (...

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Scheme 14: Proposed reaction pathway starting from 10b in the presence of ACF and silane.

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Published 23 Oct 2020

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